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Cytenamide-butyric acid (1/1)

Johnston, A., Florence, A. J., Fabbiani, F. J. A., Shankland, K. ORCID: https://orcid.org/0000-0001-6566-0155 and Bedford, C. T. (2008) Cytenamide-butyric acid (1/1). Acta Crystallographica Section E: Structure Reports Online, 64 (7). o1295-o1296. ISSN 1600-5368

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To link to this item DOI: 10.1107/S1600536808018059

Abstract/Summary

Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide-butanoic acid (1/1)], C16H13NO center dot C4H8O2. The title compound crystallizes with one molecule of cytenamide and one of butyric acid in the asymmetric unit; these molecules are linked by N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds to form an R-2(2)(8) heterodimer motif. Pairs of adjacent motifs are further connected via N-H center dot center dot center dot O interactions to form a discrete centrosymmetric assembly.

Item Type:Article
Refereed:Yes
Divisions:Life Sciences > School of Chemistry, Food and Pharmacy > School of Pharmacy
ID Code:13716
Uncontrolled Keywords:PARALLEL CRYSTALLIZATION, PACKING MOTIFS, CARBAMAZEPINE, 10,11-DIHYDROCARBAMAZEPINE, PATTERNS
Publisher:International Union of Crystallography

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