A new crystalline form of αβ-D-lactose prepared by oven drying a concentrated aqueous solution of D-lactoseNicholls, D., Elleman, C., Shankland, N. and Shankland, K. (2019) A new crystalline form of αβ-D-lactose prepared by oven drying a concentrated aqueous solution of D-lactose. Acta Crystallographica Section C - Crystal Structure Communications, 75 (7). pp. 904-909. ISSN 1600-5759
It is advisable to refer to the publisher's version if you intend to cite from this work. See Guidance on citing. To link to this item DOI: 10.1107/S2053229619008210 Abstract/SummaryA new crystalline form of αβ-D-lactose (C12H22O11, Z' = 2) has been prepared by rapid drying of an approximately 40 % w/v syrup of D-lactose. Initially identified from its novel powder X-ray diffraction pattern, the monoclinic crystal structure was solved from a microcrystal recovered from the generally polycrystalline, mixed-phase residue obtained at the end of the drying step. This is the second crystalline form of αβ-D-lactose to be identified and it has a high degree of structural 3D similarity to the previously identified triclinic form.
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