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A catemer-to-dimer structural transformation in cyheptamide

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Florence, A.J., Shankland, K., Gelbrich, T., Hursthouse, M.B., Shankland, N., Johnston, A., Fernandes, P. and Leech, C.K. (2008) A catemer-to-dimer structural transformation in cyheptamide. Crystengcomm, 10 (1). pp. 26-28. ISSN 1466-8033

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To link to this item DOI: 10.1039/b712547j

Abstract/Summary

A catemeric crystal structure of cyheptamide undergoes a transformation in the solid-state upon heating to produce a dimer-based form whose structure has been determined from laboratory X-ray powder diffraction ( XRPD) data, thereby providing the first conclusive evidence of a carbamazepine analogue crystallising in both hydrogen bonded motifs.

Item Type:Article
Refereed:Yes
Divisions:Life Sciences > School of Chemistry, Food and Pharmacy > School of Pharmacy
ID Code:13744
Uncontrolled Keywords:POWDER DIFFRACTION DATA, MOLECULAR-CRYSTAL STRUCTURES, PACKING MOTIFS, CARBAMAZEPINE, 10,11-DIHYDROCARBAMAZEPINE, CHLOROTHIAZIDE, REFINEMENT, COLLECTION
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