An optically transparent thin-layer electrochemical cell for the study of vibrational circular dichroism of chiral redox-active moleculesDomingos, S. R., Luyten, H., van Anrooij, F., Sanders, H. J., Bakker, B. H., Buma, W. J., Hartl, F. and Woutersen, S. (2013) An optically transparent thin-layer electrochemical cell for the study of vibrational circular dichroism of chiral redox-active molecules. Review of Scientific Instruments, 84 (3). 033103. ISSN 0034-6748 Full text not archived in this repository. It is advisable to refer to the publisher's version if you intend to cite from this work. See Guidance on citing. To link to this item DOI: 10.1063/1.4793722 Abstract/SummaryAn optically transparent thin-layer electrochemical (OTTLE) cell with a locally extended optical path has been developed in order to perform vibrational circular dichroism (VCD) spectroscopy on chiral molecules prepared in specific oxidation states by means of electrochemical reduction or oxidation. The new design of the electrochemical cell successfully addresses the technical challenges involved in achieving sufficient infrared absorption. The VCD-OTTLE cell proves to be a valuable tool for the investigation of chiral redox-active molecules.
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