Continuous-flow processing of gaseous ammonia using a Teflon AF-2400 tube-in-tube reactor: synthesis of thioureas and in-line titrationsBrowne, D.L., O'Brien, M., Koos, P., Cranwell, P. ORCID: https://orcid.org/0000-0001-7156-5576, Polyzos, A. and Ley, S.V. (2012) Continuous-flow processing of gaseous ammonia using a Teflon AF-2400 tube-in-tube reactor: synthesis of thioureas and in-line titrations. Synlett, 23 (9). pp. 1402-1406. ISSN 1437-2096 Full text not archived in this repository. It is advisable to refer to the publisher's version if you intend to cite from this work. See Guidance on citing. To link to this item DOI: 10.1055/s-0031-1290963 Abstract/SummaryA simple tube-in-tube reactor based on the gas-permeable membrane Teflon AF-2400 was used in the continuous flow reaction of gaseous ammonia with isothiocyanates and one isocyanate. A colourimetric in-line titration technique is also reported as a simple method to quantify the amount of ammonia taken up by the solvent in the system.
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